home *** CD-ROM | disk | FTP | other *** search
| Unknown | 1993-11-18 | 7.5 KB |
open in: 
MacOS 8.1
|
Win98
|
DOS
view JSON data
|
view as text
This file was not able to be converted.
This format is not currently supported by dexvert.
| Confidence | Program | Detection | Match Type | Support
|
|---|
| 1%
| dexvert
| Microsoft SQL Server backup (other/microsoftSQLServerBackup)
| ext
| Unsupported |
| 100%
| file
| data
| default
|
|
hex view+--------+-------------------------+-------------------------+--------+--------+
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|000014c0| 00 cc 00 18 00 00 00 00 | 00 b7 1d 00 00 00 00 00 |........|........|
|000014d0| 00 00 00 00 00 00 00 00 | 00 00 00 00 00 00 00 00 |........|........|
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|000014f0| 2e 33 33 00 30 2e 33 33 | 00 30 2e 33 33 00 02 00 |.33.0.33|.0.33...|
|00001500| 00 00 37 00 28 53 29 2d | 28 2d 2d 29 2d 44 69 6d |..7.(S)-|(--)-Dim|
|00001510| 65 74 68 79 6c 2d 6d 61 | 6c 61 74 20 61 75 73 20 |ethyl-ma|lat aus |
|00001520| 28 53 29 2d 32 2d 48 79 | 64 72 6f 78 79 62 65 72 |(S)-2-Hy|droxyber|
|00001530| 6e 73 74 65 69 6e 73 e4 | 75 72 65 b5 00 33 38 2e |nsteins.|ure..38.|
|00001540| 38 20 67 20 28 32 34 30 | 20 6d 6d 6f 6c 29 20 09 |8 g (240| mmol) .|
|00001550| 28 53 29 2d 32 2d 48 79 | 64 72 6f 78 79 62 65 72 |(S)-2-Hy|droxyber|
|00001560| 6e 73 74 65 69 6e 73 e4 | 75 72 65 0d 0a 35 30 30 |nsteins.|ure..500|
|00001570| 20 6d 6c 20 09 09 54 48 | 46 20 28 61 62 73 6f 6c | ml ..TH|F (absol|
|00001580| 75 74 29 0d 0a 32 34 2e | 34 20 6d 6c 20 28 32 34 |ut)..24.|4 ml (24|
|00001590| 34 20 6d 6f 6c 29 20 09 | 42 6f 72 61 6e 2d 64 69 |4 mol) .|Boran-di|
|000015a0| 6d 65 74 68 79 6c 2d 73 | 75 6c 64 66 69 64 2d 4b |methyl-s|uldfid-K|
|000015b0| 6f 6d 70 6c 65 78 20 28 | 42 4d 53 29 0d 0a 30 2e |omplex (|BMS)..0.|
|000015c0| 34 20 67 20 28 31 32 20 | 6d 6d 6f 6c 29 20 09 4e |4 g (12 |mmol) .N|
|000015d0| 61 74 72 69 75 6d 62 6f | 72 68 79 64 72 69 64 0d |atriumbo|rhydrid.|
|000015e0| 0a 31 34 34 20 6d 6c 20 | 09 09 4d 65 74 68 61 6e |.144 ml |..Methan|
|000015f0| 6f 6c 42 00 20 31 30 30 | 30 20 6d 6c 20 44 72 65 |olB. 100|0 ml Dre|
|00001600| 69 68 61 6c 73 6b 6f 6c | 62 65 6e 20 6d 69 74 20 |ihalskol|ben mit |
|00001610| 53 74 69 63 6b 73 74 6f | 66 66 62 61 6c 6c 6f 6e |Sticksto|ffballon|
|00001620| 2c 20 54 68 65 72 6d 6f | 6d 65 74 65 72 2c 20 53 |, Thermo|meter, S|
|00001630| 65 70 74 75 6d 2e dc 01 | 44 69 65 20 4c f6 73 75 |eptum...|Die L.su|
|00001640| 6e 67 20 64 65 72 20 42 | 65 72 6e 73 74 65 69 6e |ng der B|ernstein|
|00001650| 73 e4 75 72 65 20 69 6e | 20 61 62 73 6f 6c 75 74 |s.ure in| absolut|
|00001660| 65 6d 20 54 48 46 20 77 | 69 72 64 20 62 65 69 20 |em THF w|ird bei |
|00001670| 35 b0 43 20 20 76 6f 72 | 67 65 6c 65 67 74 2c 20 |5.C vor|gelegt, |
|00001680| 64 61 73 20 42 4d 53 20 | 64 61 7a 75 67 65 67 65 |das BMS |dazugege|
|00001690| 62 65 6e 20 75 6e 64 20 | 30 2e 35 20 68 20 62 65 |ben und |0.5 h be|
|000016a0| 69 20 52 54 20 67 65 72 | fc 68 72 74 2e 20 45 73 |i RT ger|.hrt. Es|
|000016b0| 20 6c e4 df 74 20 73 69 | 63 68 20 65 69 6e 65 20 | l..t si|ch eine |
|000016c0| 47 61 73 65 6e 74 77 69 | 63 6b 6c 75 6e 67 20 62 |Gasentwi|cklung b|
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|000016e0| 69 65 df 65 6e 64 20 77 | 69 72 64 20 61 75 66 20 |ie.end w|ird auf |
|000016f0| 35 b0 43 20 68 65 72 75 | 6e 74 65 72 67 65 6b fc |5.C heru|ntergek.|
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|00001710| 34 20 64 61 7a 75 67 65 | 67 65 62 65 6e 2e 0d 0a |4 dazuge|geben...|
|00001720| 4d 61 6e 20 6c e4 df 74 | 20 64 69 65 20 4d 69 73 |Man l..t| die Mis|
|00001730| 63 68 75 6e 67 20 6c 61 | 6e 67 73 61 6d 20 61 75 |chung la|ngsam au|
|00001740| 66 20 52 54 20 6b 6f 6d | 6d 65 6e 20 75 6e 64 20 |f RT kom|men und |
|00001750| 72 fc 68 72 74 20 31 20 | 68 2c 20 61 6e 73 63 68 |r.hrt 1 |h, ansch|
|00001760| 6c 69 65 df 65 6e 64 20 | 77 69 72 64 20 64 61 73 |lie.end |wird das|
|00001770| 20 4d 65 74 68 61 6e 6f | 6c 20 64 61 7a 75 67 65 | Methano|l dazuge|
|00001780| 67 65 62 65 6e 20 75 6e | 64 20 64 69 65 20 4d 69 |geben un|d die Mi|
|00001790| 73 63 68 75 6e 67 20 fc | 62 65 72 20 4e 61 63 68 |schung .|ber Nach|
|000017a0| 74 20 67 65 72 fc 68 72 | 74 2e 20 44 61 73 20 53 |t ger.hr|t. Das S|
|000017b0| 6f 6c 76 65 6e 73 20 77 | 69 72 64 20 61 6d 20 0d |olvens w|ird am .|
|000017c0| 0a 52 6f 74 61 74 69 6f | 6e 73 76 65 72 64 61 6d |.Rotatio|nsverdam|
|000017d0| 70 66 65 72 20 61 62 67 | 65 7a 6f 67 65 6e 2e 20 |pfer abg|ezogen. |
|000017e0| 0d 0a 44 69 65 20 52 65 | 69 6e 69 67 75 6e 67 20 |..Die Re|inigung |
|000017f0| 65 72 66 6f 6c 67 74 20 | 64 75 72 63 68 20 4b 75 |erfolgt |durch Ku|
|00001800| 67 65 6c 72 6f 68 72 64 | 65 73 74 69 6c 6c 61 74 |gelrohrd|estillat|
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|00001820| 61 72 29 23 00 36 33 20 | 28 65 6e 74 73 70 72 69 |ar)#.63 |(entspri|
|00001830| 63 68 74 20 20 32 30 2c | 34 20 67 20 28 31 35 32 |cht 20,|4 g (152|
|00001840| 20 6d 6d 6f 6c 29 20 29 | 4a 00 56 65 72 73 63 68 | mmol) )|J.Versch|
|00001850| 69 65 62 75 6e 67 65 6e | 3a 09 32 2e 34 35 20 28 |iebungen|:.2.45 (|
|00001860| 64 2c 20 32 48 29 0d 0a | 09 09 33 2e 36 35 20 28 |d, 2H)..|..3.65 (|
|00001870| 64 2c 20 32 48 29 0d 0a | 09 09 33 2e 36 20 28 73 |d, 2H)..|..3.6 (s|
|00001880| 2c 20 33 48 29 0d 0a 09 | 09 34 2e 32 20 28 6d 2c |, 3H)...|.4.2 (m,|
|00001890| 20 31 48 29 33 00 41 6e | 6d 65 72 6b 75 6e 67 3a | 1H)3.An|merkung:|
|000018a0| 20 44 61 73 20 53 70 65 | 6b 74 72 75 6d 20 7a 65 | Das Spe|ktrum ze|
|000018b0| 69 67 74 20 64 69 65 20 | 65 72 77 61 72 74 65 74 |igt die |erwartet|
|000018c0| 65 6e 20 50 65 61 6b 73 | 2e 27 00 43 48 45 4d 49 |en Peaks|.'.CHEMI|
|000018d0| 53 54 52 59 20 4c 45 54 | 54 45 52 53 2c 20 70 70 |STRY LET|TERS, pp|
|000018e0| 2e 20 31 33 38 39 2d 2d | 31 33 39 32 2c 20 31 39 |. 1389--|1392, 19|
|000018f0| 38 34 09 00 63 68 65 6d | 31 2e 62 6d 70 02 00 33 |84..chem|1.bmp..3|
|00001900| 33 00 00 00 00 00 00 00 | 00 00 00 00 00 00 00 00 |3.......|........|
|00001910| 00 00 00 00 00 00 00 00 | 00 00 00 00 00 00 00 00 |........|........|
|00001920| 00 00 00 00 00 00 00 00 | 00 00 00 55 00 44 61 72 |........|...U.Dar|
|00001930| 73 74 65 6c 6c 75 6e 67 | 20 76 6f 6e 20 32 2c 32 |stellung| von 2,2|
|00001940| 2d 44 69 6d 65 74 68 79 | 6c 2d 31 2c 33 2d 44 69 |-Dimethy|l-1,3-Di|
|00001950| 6f 78 6f 6c 61 6e 2d 34 | 2d 6d 65 74 68 79 6c 61 |oxolan-4|-methyla|
|00001960| 63 65 74 61 74 20 61 75 | 73 20 28 53 29 2d 28 2d |cetat au|s (S)-(-|
|00001970| 2d 29 2d 44 69 6d 65 74 | 68 79 6c 2d 6d 61 6c 61 |-)-Dimet|hyl-mala|
|00001980| 74 20 94 00 32 30 2e 34 | 20 67 20 28 31 35 32 20 |t ..20.4| g (152 |
|00001990| 6d 6d 6f 6c 29 20 09 09 | 28 53 29 2d 28 2d 2d 29 |mmol) ..|(S)-(--)|
|000019a0| 2d 44 69 6d 65 74 68 79 | 6c 2d 6d 61 6c 61 74 0d |-Dimethy|l-malat.|
|000019b0| 0a 32 30 30 20 6d 6c 20 | 09 09 09 43 48 32 43 6c |.200 ml |...CH2Cl|
|000019c0| 32 20 28 61 62 73 6f 6c | 75 74 29 0d 0a 31 30 30 |2 (absol|ut)..100|
|000019d0| 20 6d 67 20 09 09 09 70 | 2d 54 6f 6c 75 6f 6c 73 | mg ...p|-Toluols|
|000019e0| 75 6c 66 6f 6e 73 e4 75 | 72 65 0d 0a 31 32 20 67 |ulfons.u|re..12 g|
|000019f0| 20 28 30 2e 31 36 37 20 | 6d 6f 6c 29 20 09 09 32 | (0.167 |mol) ..2|
|00001a00| 2d 4d 65 74 68 79 6c 2d | 6d 65 74 68 79 6c 76 69 |-Methyl-|methylvi|
|00001a10| 6e 79 6c 65 74 68 65 72 | 41 00 20 35 30 30 20 6d |nylether|A. 500 m|
|00001a20| 6c 20 44 72 65 69 68 61 | 6c 73 6b 6f 6c 62 65 6e |l Dreiha|lskolben|
|00001a30| 20 6d 69 74 20 53 74 69 | 63 6b 73 74 6f 66 66 62 | mit Sti|ckstoffb|
|00001a40| 61 6c 6c 6f 6e 2c 20 54 | 68 65 72 6d 6f 6d 65 74 |allon, T|hermomet|
|00001a50| 65 72 2c 20 53 65 70 74 | 75 6d 2e db 01 44 69 65 |er, Sept|um...Die|
|00001a60| 20 4c f6 73 75 6e 67 20 | 64 65 73 20 56 69 6e 79 | L.sung |des Viny|
|00001a70| 6c 65 74 68 65 72 73 2f | 70 2d 54 53 20 69 6e 20 |lethers/|p-TS in |
|00001a80| 61 62 73 6f 6c 75 74 65 | 6d 20 4d 65 74 68 79 6c |absolute|m Methyl|
|00001a90| 65 6e 63 68 6c 6f 72 69 | 64 20 77 69 72 64 20 62 |enchlori|d wird b|
|00001aa0| 65 69 20 30 b0 43 20 76 | 6f 72 67 65 6c 65 67 74 |ei 0.C v|orgelegt|
|00001ab0| 2c 20 64 61 73 20 4d 61 | 6c 61 74 20 2d 2d 20 6d |, das Ma|lat -- m|
|00001ac0| 69 74 20 43 48 32 43 6c | 32 20 76 65 72 64 fc 6e |it CH2Cl|2 verd.n|
|00001ad0| 6e 74 20 2d 2d 20 6d 69 | 74 74 65 6c 73 20 53 65 |nt -- mi|ttels Se|
|00001ae0| 70 74 75 6d 20 75 6e 64 | 20 53 70 72 69 74 7a 65 |ptum und| Spritze|
|00001af0| 20 64 61 7a 75 67 65 67 | 65 62 65 6e 20 75 6e 64 | dazugeg|eben und|
|00001b00| 20 31 20 68 20 67 65 72 | fc 68 72 74 2e 0d 0a 4d | 1 h ger|.hrt...M|
|00001b10| 61 6e 20 20 6c e4 df 74 | 20 64 69 65 20 4d 69 73 |an l..t| die Mis|
|00001b20| 63 68 75 6e 67 20 61 75 | 66 20 52 54 20 6b 6f 6d |chung au|f RT kom|
|00001b30| 6d 65 6e 20 75 6e 64 20 | 72 fc 68 72 74 20 77 65 |men und |r.hrt we|
|00001b40| 69 74 65 72 65 20 31 35 | 20 6d 69 6e 2e 2c 20 61 |itere 15| min., a|
|00001b50| 6e 73 63 68 6c 69 65 df | 65 6e 64 20 77 69 72 64 |nschlie.|end wird|
|00001b60| 20 6d 69 74 20 67 65 73 | 2e 20 4e 61 43 6c 2d 4c | mit ges|. NaCl-L|
|00001b70| f6 73 75 6e 67 20 67 65 | 77 61 73 63 68 65 6e 20 |.sung ge|waschen |
|00001b80| 75 6e 64 20 64 61 73 20 | 50 72 6f 64 75 6b 74 20 |und das |Produkt |
|00001b90| 69 6d 20 53 63 68 fc 74 | 74 65 6c 74 72 69 63 68 |im Sch.t|teltrich|
|00001ba0| 74 65 72 20 6d 69 74 20 | 43 48 32 43 6c 32 20 65 |ter mit |CH2Cl2 e|
|00001bb0| 78 74 72 61 68 69 65 72 | 74 2e 0d 0a 44 61 73 20 |xtrahier|t...Das |
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|00001df0| 00 00 00 00 | |.... | |
+--------+-------------------------+-------------------------+--------+--------+
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